Diastereodivergent reverse prenylation of indole and tryptophan derivatives:total synthesis of amauromine, novoamauromine, and epi-amauromine

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Autor/in:
Erscheinungsjahr:
2016
Medientyp:
Text
Schlagworte:
  • alkaloids
  • diastereodivergent reactions
  • iridium
  • prenylation
  • total synthesis
Beschreibung:
  • A regio- and stereoselective reverse prenylation of indole and tryptophan derivatives is presented. All four possible stereoisomers are accessible through this iridium-catalyzed reaction. The stereoselectivity is controlled by a chiral phosphoramidite ligand in combination with an achiral borane additive and can be switched by changing the nature of the borane. One enantiomer of the ligand is thus sufficient to prepare all possible isomers. The synthetic potential of this method was demonstrated by a short total synthesis of amauromine and its two natural diastereomers.
Lizenz:
  • info:eu-repo/semantics/closedAccess
Quellsystem:
Forschungsinformationssystem der UHH

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Quelldatensatz
oai:www.edit.fis.uni-hamburg.de:publications/6c8c985e-d4e9-4ec8-b70a-2a80299e3f2d