Visible-Light Photolysis of Allyl Zirconocenes: A Photoinduced Three-Component Radical (4+2)-Cyclization-Allylation Reaction

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Autor/in:
Erscheinungsjahr:
2017
Medientyp:
Text
Schlagworte:
  • Radicals
  • Alkenes
  • Unactivated alkenes
  • Catalysis
  • Synthesis (Chemical)
  • Catalysts
  • Radicals
  • Alkenes
  • Unactivated alkenes
  • Catalysis
  • Synthesis (Chemical)
  • Catalysts
Beschreibung:
  • A photoinduced, three-component radical (4+2)-cyclization-allylation reaction between 3-(2-iodoethyl) indoles, acceptor-substituted alkenes, and allyl zirconocenes of the structure Cp2ZrCl(sigma-allyl) was developed. The protocol leads to highly functionalized hexahydro-carbazoles in a single step, establishing three C-C bonds and three contiguous stereocenters at once. The radical reaction is initiated by direct photolysis of allyl zirconocenes to generate free allyl radicals.
Lizenz:
  • info:eu-repo/semantics/restrictedAccess
Quellsystem:
Forschungsinformationssystem der UHH

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Quelldatensatz
oai:www.edit.fis.uni-hamburg.de:publications/86c083c5-939c-44d3-a209-749e466d7656