Characterization of picomole amounts of oligosaccharides from glycoproteins by1H NMR spectroscopy

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Autor/in:
Erscheinungsjahr:
2010
Medientyp:
Text
Schlagworte:
  • Molecular Dynamics Simulation
  • Carbohydrates
  • Glycosidic linkage
  • Glycosylation
  • Glycosides
  • Structural reporter groups
  • Glycoproteins
  • Oligosaccharides
  • NMR spectroscopy
  • Water suppression
  • Molecular Dynamics Simulation
  • Carbohydrates
  • Glycosidic linkage
  • Glycosylation
  • Glycosides
Beschreibung:
  • (Graph Presented) Can you see it? NMR spectroscopy is indispensible for structure analysis. It is believed that its use is limited if less than several nanomoles are available. The characterization of oligosaccharides as components of glycoproteins by NMR spectroscopy utilizing significantly less material is highly desirable. Optimization of the sample preparation, water suppression, and instrument setup has enabled only 15 picomoles of oligosaccharides to be analyzed by NMR spectroscopy. © 2010 Wiley-VCH Verlag GmbH & Co. KGaA.
Lizenz:
  • info:eu-repo/semantics/restrictedAccess
Quellsystem:
Forschungsinformationssystem der UHH
Interne Metadaten
Quelldatensatz
oai:www.edit.fis.uni-hamburg.de:publications/813d6956-cba3-4481-8a42-4a66c151d354