Thermal behaviour of crystal and domain structure of LSGMn-05 anode material for SOFC

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Autor/in:
Erscheinungsjahr:
2013
Medientyp:
Text
Schlagworte:
  • Avalanches
  • Domain walls
  • Twin walls
  • Phase Transitions
  • Ferroelectric Materials
  • Ferroelectricity
  • Avalanches
  • Domain walls
  • Twin walls
  • Phase Transitions
  • Ferroelectric Materials
  • Ferroelectricity
Beschreibung:
  • The structure of perovskite-type La0.95Sr0.05Ga0.95Mn0.05O3-x crystals has been investigated using high-resolution X-ray powder diffraction technique in the temperature range of 298-1173 K. A transition from orthorhombic (Pbnm) to rhombohedral (R (3) over barc) phase has been detected near 340 K. A chevron-like configuration of ferroelastic domain structure was observed in rhombohedral La0.95Sr0.05Ga0.95Mn0.05O3-x crystal using the Laue technique. The chevron-like pattern is formed by the intersection of W-type domain walls (211), (101) and (110) and demonstrates the reversibility of this domain wall structure configuration at thermal cycling through the phase transition point.
Lizenz:
  • info:eu-repo/semantics/restrictedAccess
Quellsystem:
Forschungsinformationssystem der UHH

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oai:www.edit.fis.uni-hamburg.de:publications/5e1745c9-98b9-46b5-89a3-063fd1536fa2